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DOI: dx.doi/10.18535/ijetst/v3i04.07. Synthesis and Characterization of Copper Nanoparticles, Using. Combination of Two Different Sizes of Balls in Wet Ball Milling. Authors. Shravan Kumar Yadav. 1. , Dr V. Vasu. 2. 1,2. Mechanical Engineering Department, National Institute of Technology Warangal, India. Email:.
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A solvent-free method for the Sonogashira coupling reaction was established under ball milling conditions without the use of copper or additional ligands. Pd(OAc)2 or Pd(PPh3)4 in combination with 1,4-diazabicyclo[2.2.2]octane (DABCO) were chosen as catalysts and base, respectively. The reaction was investigated us.
Dry ball milling of hexosides with trityl chloride in the presence of DABCO or Na2CO3 has been found to result in their complete conversion to the respective 6‐O‐trityl ethers. Further wet grinding of the reaction mixture with Ac2O in the presence of DMAP led to the respective fully protected hexosides in good to excellent.
GENERAL PAPERS. Performance optimization of an industrial ball mill for chromite processing. S.K. TripathyI; Y.R. MurthyI; V. SinghI; A. SrinivasuluII; A. RanjanII; P.K. SatijaII. IResearch and Development Department, Tata Steel Ltd. Jamshedpur, India IIFerro Alloys Minerals Division, Tata Steel Ltd. Sukinda, India.
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in a Fritsch P-5 planetary ball mill using chrome steel vials and balls in order synthesize nanostructured elemental Cu. electron microscopy, eds and x-ray diffraction. SEM analysis was performed to study the microstructure and bonding between the matrix and the reinforcement. A. JEOL JSM-6480LV scanning electron.